Calcitriol_Impurities_A_RP-HPLC_11856_MedChemExpress

Data File C:\\CHEM32\\2\\DATA\\20170728\\20170728 2017-07-28 08-57-10\\001-0101.DSample Name: BLANK=====================================================================Acq. Operator : ZLL Seq. Line : 1Acq. Instrument : HPLC-12 Location : Vial 1Injection Date : 2017-07-28 08:58:44 Inj : 1 Inj Volume : 10.0 µlAcq. Method : C:\\CHEM32\\2\\DATA\\20170728\\20170728 2017-07-28 08-57-10\\55,230NM.MLast changed : 2017-07-28 08:44:25 by ZLL Analysis Method : C:\\CHEM32\\2\\METHODS\\55,230NM.MLast changed : 2017-07-28 10:34:10 by ZLL (modified after loading)Catalog No : HY-75041 Batch#11856 BLANK A-RP-200 Additional Info : Peak(s) manually integrated DAD1 D, Sig=230,4 Ref=360,100 (20170728\\20170728 2017-07-28 08-57-10\\001-0101.D)mAU5004003002001000-1000510152025min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier: : 1.0000Dilution: : 1.0000Use Multiplier & Dilution Factor with ISTDs No peaks found ===================================================================== *** End of Report ***HPLC-12 2017-07-28 10:34:12 ZLL Page 1 of 1

Data File C:\\CHEM32\\2\\DATA\\20170728\\20170728 2017-07-28 09-56-08\\074-0101.DSample Name: CPK2017-727-11856=====================================================================Acq. Operator : ZLL Seq. Line : 1Acq. Instrument : HPLC-12 Location : Vial 74Injection Date : 2017-07-28 09:58:03 Inj : 1 Inj Volume : 10.0 µlDifferent Inj Volume from Sequence ! Actual Inj Volume : 25.0 µlAcq. Method : C:\\CHEM32\\2\\DATA\\20170728\\20170728 2017-07-28 09-56-08\\55,230NM.MLast changed : 2017-07-28 08:44:25 by ZLL Analysis Method : C:\\CHEM32\\2\\METHODS\\55,230NM.MLast changed : 2017-07-28 02:28:16 by ZLL (modified after loading)Catalog No : HY-75041 Batch#11856 A-RP-200 Additional Info : Peak(s) manually integrated DAD1 D, Sig=230,4 Ref=360,100 (20170728\\20170728 2017-07-28 09-56-08\\074-0101.D) 13.448 10.325 10.980 12.052 3.945 5.225 7.159 14.773mAU2502001501005000510152025min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier: : 1.0000Dilution: : 1.0000Use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 D, Sig=230,4 Ref=360,100 Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 3.945 MM R 0.2143 11.400 8.90702e-1 0.1560 2 5.225 BV 0.1269 4.06518 4.70107e-1 0.05 3 7.159 BV 0.2805 11.55834 5.38396e-1 0.1574 4 10.325 BB 0.2537 14.04247 7.81163e-1 0.1912 5 10.980 BB 0.2975 14.88186 5.956e-1 0.2027 6 12.052 BB 0.2457 6.82001 3.52571e-1 0.0929 7 13.448 BB 0.3531 7024.47021 309.048 95.6615 8 14.773 BB 0.4393 255.75853 8.35128 3.4830 Totals : 7343.05061 321.06935 ===================================================================== *** End of Report ***HPLC-12 2017-07-28 02:31:51 ZLL Page 1 of 1